Importance
of Testing Cement before Construction
These different methods for testing
the strength of Cement are important to ensure that the Cement used in
construction meets the necessary standards and is able to perform its intended
function.
Testing Cement before construction
is important for several reasons:
Quality assurance: Cement tests ensure that the Cement used in construction
meets the necessary quality standards. It helps to ensure that the Cement is of
the required strength, durability, and other properties necessary for its
intended use.
Safety: Cement tests ensure that the Cement used in construction is
safe for use. It helps to prevent accidents and failures that could occur due
to the use of substandard Cement.
Cost-effectiveness: Testing Cement helps to make sure that the right quantity of
Cement is used for a particular application. This can help to avoid wastage and
reduce costs.
Durability: Testing Cement helps to ensure that the Cement used in
construction is durable and able to withstand the intended load and
environmental conditions.
Compliance: Cement tests help to make sure that the Cement used in
construction complies with relevant industry standards and regulations. This is
important for ensuring that the construction project meets legal requirements
and is safe for use.
In summary, testing Cement before
construction is important for ensuring the quality, safety, cost-effectiveness,
durability, and compliance of the construction project. It is a necessary step
in the construction process that should not be overlooked.
DETERMINATION
OF FINENESS OF CEMENT BY SIEVIE
Theory:
Cement is obtained by grinding various raw materials after calcinations.
The degree to which cement is ground to smaller and smaller particles is called
fineness of cement. The fineness of cement has an important role on the rate of
hydration and hence on the rate of gain of strength and also on the rate of
evolution of heat. Finer cement offers a greater surface area for hydration and
hence the faster development of strength although the ultimate strength is not
affected. Fineness also provides more cohesiveness to concrete and avoid
separation of water at the top of concrete (called bleeding). However, increase
in fineness of cement increases the drying shrinkage and cracking of the
concrete. Fineness of cement is tested either by sieving or by determination of
specific surface using air-permeability apparatus. The specific surface is
defined as the total surface area of all the particles in cm² per one gram of cement. Although
determination of specific surface is more accurate to judge fineness of cement,
it is rarely used except for specific purpose. In contrast sieving is most
commonly used method to determine fineness of cement and is quite good for
field works.
Objective: Determination of fineness of cement by dry sieving. Reference: IS 4031 (Part-1):1988. Apparatus: IS-90 micron sieve conforming to IS: 460 (Part 1-3)-1985; Weighing balance; Gauging trowel; Brush. Material: Ordinary Portland cement
Procedure: 1. Weigh accurately 100 g of cement to the nearest 0.01 g and place it on a standard 90 micron IS sieve.
2. Break down any air-set lumps in the cement sample with fingers.
3. Agitate the sieve by giving swirling, planetary and linear movements for a period of 10 minutes or until no more fine material passes through it.
4. Collect the residue left on the sieve, using brush if necessary, and weigh the residue.
5. Express the residue as a percentage of the quantity first placed on the sieve to the nearest 0.1 percent.
6. Repeat the whole procedures two more times each using fresh 100 g sample. 2
Observations:
Sl. No |
Weight of
sample taken (W) (in g.) |
Weight of
residue (R) (in g.) |
%age of residue = 𝑅 ̸ 𝑊 × 100 |
Average % of residue |
1 |
|
|
|
|
2 |
|
|
|
|
3 |
|
|
|
|
4 |
|
|
|
|
Result: Percentage residue of cement sample by dry sieving is ___________ percentage.
Conclusions: The given sample of cement contains less than/ more than 10% by weight of material coarser than 90 micron sieve.
Therefore it satisfies/ not satisfies the criterion as specified by IS code. Precautions:
Discuss about the precautions to be taken while conducting this experiment
ADVANCE STUDY/KNOWLEDGE
The fineness of cement has a direct
impact on the rate of hydration. Finer cement particles have a greater surface
area, which allows for faster chemical reactions between the cement and water
during the hydration process.
Specifically:
Finer cement particles have a larger
surface area per unit volume compared to coarser particles. This increased
surface area provides more sites for the hydration reactions to take place.
·
The faster hydration of finer cement
allows for quicker development of strength in the early stages of cement
setting and hardening. The higher surface area accelerates the initial chemical
reactions.
·
Finer cement also results in a more
homogeneous and dense hydration product distribution within the cement paste.
This improves the overall strength and durability of the hardened cement.
·
However, excessively fine cement can
also lead to challenges, such as increased water demand, higher heat of
hydration, and increased risk of drying shrinkage. There is an optimal fineness
range for cement based on the intended application.
In summary, increasing the fineness
of cement generally increases the rate of hydration, leading to faster initial
strength gain, but must be balanced against potential drawbacks of very fine
cement particles.
Advantages and disadvantages of
Fineness of Cement
The disadvantage of high fineness, include: - The cost of grinding to a higher fineness is considerable. - The finer the cement the more rapidly it deteriorates on exposure to the atmosphere during bad storage. - Finer cement increases the surface area of its alkalis – leads to stronger reaction with alkali- reactive aggregate – cracks and deterioration of concrete. - Finer cement exhibits a higher shrinkage and a greater proneness to cracking. - An increase in fineness increases the amount of gypsum required for proper retardation because, in finer cement, more C3A is available for early hydration (due to the increase of its surface area). Fineness of cement is tested in two ways:
(a) By sieving.
(b) By determination of specific surface (total surface area of all the particles in one gram of cement) by air-permeability apparatus. Expressed as cm² /gm or m² /kg.
Generally Blaine Air permeability apparatus is used.
a) By sieving: Weigh correctly 100 grams of cement and take it on a standard IS Sieve No. 9 -90 µ microns). Break down the air-set lumps in the sample with fingers. Continuously sieve the sample giving circular and vertical motion for a period of 15 minutes. Mechanical sieving devices may also be used. Weigh the residue left on the sieve. This weight shall not exceed 10% for ordinary cement. Sieve test is rarely used due to clogging sieves opens with cements particles.
b) By Blaine test Principle of this method is in observing the time taken for a fixed quantity of air to flow through compacted cement bed of specified dimension and porosity. Volume of cement bed in the cell can be found by it with mercury before and after putting cement on it then determine the difference between two weights, this difference divided by mercury density in room temperature to obtain volume of cement bed. Repeat this for twice at least and use the average value of volume in following equations, also the weight of cement used in cell must be with porosity equal to 0.5 ± 0.0005.
W= 3.15 V ( 1 – e )
Which: 3.15 = specific gravity of cement W= weight of cement V = volume of cement bed e = porosity of cement bed Place the perforated disc on the ledge at the bottom of the cell and place on it a new filter paper disc. Place the sample of standard cement weighted (W) with knowing surface area, in the cell. Place a second new filter paper disc on the levelled cement. Insert the plunger and press it gently but firmly until the lower face of the cap is in contact with the cell. Then air pumped inside the tube raise the level of the manometer liquid to that of the highest etched line. Close the stopcock and the manometer liquid will begins to flow. Start the timer as the liquid reaches the second etched line and stop it when the liquid reaches the third etched line. Record the time, t .The procedure repeats three times for standard sample and tested one. The surface area then can be calculated by Which: S = specific area of tested cement sample ( cm² \gm) Ss = specific area of standard cement ( cm² \gm ) T = average time for tested sample Ts = average time for standard sample.
Correction
factor of a sieve
A correction factor is a factor multiplied with the result of an equation to correct for a known amount of systemic error.
Although many numerical evaluations are likely to be precise, you may not always arrive at a specific conclusion in terms of measurements. This is because multiple factors can come into play, resulting in skewed conclusions. Oftentimes the need for evaluating these uncertain factors is a necessity.
This process of evaluating factors that lead to uncertainty in measurement results is known as uncertainty evaluation or error analysis. Error analysis is dependent on correction factors, which are designated calculations implemented to evaluate uncertain factors in measured results
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